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New Carbon-Hydrogen Activating Metal Complexes

New Carbon-Hydrogen Activating Metal Complexes

Alexander Krajete (ORCID: )
  • Grant DOI 10.55776/J2223
  • Funding program Erwin Schrödinger
  • Status ended
  • Start November 18, 2002
  • End November 18, 2003
  • Funding amount € 35,300

Disciplines

Chemistry (100%)

Keywords

    Alkanes, Late Transition Metal Complexes, Carbon-Hydrogen Activation, Stoichiometric C-H Activation, Ligands, Catalytic C-H Activation

Abstract

Chemistry is the science about breaking and forming of bonds between atoms. One of the most important challenges of todays chemistry is the selective breaking of carbon-hydrogen bonding in combination with further functionalization into useful products, especially in saturated and unreactive hydrocarbons like alkanes, the main constituents of oil and natural gas. The major goal of this project is the development and characterization of new ligands and their usage for the preparation of new half sandwich complexes bearing hemilabile ligands like carbon monoxide or phosphines as potential precursors for C-H activation reactions. The project consists of 3 major synthetic parts: 1. Synthesis of new trisiminoborate ligands being sterically more demanding with possibly higher stabilizing power (compared to established and nearly exclusively used pentamethylcyclopentadienyl and tripyrazolylborate systems). 2. Synthesis of new carbonyl and/or carbonyl/phosphine containing mixed transition metal complexes (d9 metal rhodium preferred) with reported dienyl and carborane ligands being both sterically more demanding in combination with higher stabilizing capability. 3. Application of new complexes with tailored ligand design to stoichiometric C-H- (detection and isolation of alkyl hydride complexes) and the extension to the most challenging catalytic C-H activation with direct functionalization into synthetically useful products. The recent reported catalytic systems highlight the potential of organometallic chemistry for useful C-H bond activation with far reaching economical consequences that will ultimatively allow us to exploit Earths alkane resources more efficiently and cleanly.

Research institution(s)
  • University of California Berkeley - 100%
  • Universität Innsbruck - 10%

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